Sigma-Aldrich
Methanol-D3 99.8 atom % D, 5 grams
- Part Number:
- MIL-343854-5G
- Lead Time:
- 2-4 weeks
- Minimum Purchase:
- 1 unit
- Shipping:
- FREE SHIPPING on most orders over $50*
- Quantity:
- each
- Size:
- 5 grams
- Style:
- chemical
- DOT Rated:
- HazMat Transport Fee Required
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Description
Methanol-D3 99.8 Atom% D 5 Grams
Synonym: 1,1,1-Trideuteromethanol, Methyl-d3 alcohol
- CAS Number 2219-52-5
- Linear Formula DOCH2CH2OD
- Molecular Weight 64.08
- MDL number MFCD00075277
- PubChem Substance ID 24861206
- NACRES NA.21
Quality Level | 200 |
Isotopic Purity | 99.8 atom % D |
Assay | 99% (CP) |
Expl. Lim. | 5.5-36.5 % |
Impurities | ≤0.05% water |
Refractive Index | n20/D 1.327 (lit.) |
bp | 65°C (lit.) |
Density | 0.867 g/mL at 25°C (lit.) |
Mass Shift | M+3 |
General description
Methanol-d3 is a deuterated NMR solvent that is useful in NMR-based research and analyses.
Application
Methanol-d3 may be used in the preparation of [Al(CH3)2OCD3]3 by reacting with trimethylaluminum for use in spectroscopic analysis of dialkylaluminum alkoxides and the trialkylaluminum-ether complex.
Safety Information
Signal word Danger
Hazard statements H225-H301 + H311 + H331-H370
Precautionary statements P210-P260-P280-P301 + P310 + P330-P308 + P311-P403 + P233
Personal Protective Equipment Eyeshields, Faceshields, Full-face respirator (US), Gloves, Multi-purpose combination respirator cartridge (US)
RIDADR UN1230 - class 3 - PG 2 - Methanol
WGK Germany 1
Flash Point(F) 51.8°F
Flash Point(C) 11°C
Documents
Warnings
Note: These chemicals are for research & laboratory use only. Your order will not be processed if you do not work for, and ship to, a registered laboratory or research facility. Not for topical applications. An official Declaration of Use form may be required.
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WARNING: This product can expose you to chemicals which are known to the State of California to cause cancer and reproductive harm. Prop 65 Warning
Please note: This product is not returnable.
General description Cyclohexane undergoes oxidation in the presence of various oxidants such as hydrogen peroxide, tert-butyl hydroperoxide and molecular oxygen.[2]
Application Cyclohexane has been used to prepare a 1.3M solution of sec-butyllithium.[3] It may be used as a starting Reagent for the synthesis of adipic acid[1] and ε-caprolactam.[1]