Sigma-Aldrich

Methanol-D3 99.8 atom % D, 5 grams

Part Number:
MIL-343854-5G
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2-4 weeks
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1 unit
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Size:
5 grams
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Price: $329.28

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Description

Methanol-D3 99.8 Atom% D 5 Grams

Synonym: 1,1,1-Trideuteromethanol, Methyl-d3 alcohol

  • CAS Number 2219-52-5
  • Linear Formula DOCH2CH2OD
  • Molecular Weight 64.08
  • MDL number MFCD00075277
  • PubChem Substance ID 24861206
  • NACRES NA.21
Quality Level 200
Isotopic Purity 99.8 atom % D
Assay 99% (CP)
Expl. Lim. 5.5-36.5 %
Impurities ≤0.05% water
Refractive Index n20/D 1.327 (lit.)
bp 65°C (lit.)
Density 0.867 g/mL at 25°C (lit.)
Mass Shift M+3

General description
Methanol-d3 is a deuterated NMR solvent that is useful in NMR-based research and analyses.

Application
Methanol-d3 may be used in the preparation of [Al(CH3)2OCD3]3 by reacting with trimethylaluminum for use in spectroscopic analysis of dialkylaluminum alkoxides and the trialkylaluminum-ether complex.

Safety Information

Signal word Danger
Hazard statements H225-H301 + H311 + H331-H370
Precautionary statements P210-P260-P280-P301 + P310 + P330-P308 + P311-P403 + P233
Personal Protective Equipment Eyeshields, Faceshields, Full-face respirator (US), Gloves, Multi-purpose combination respirator cartridge (US)
RIDADR UN1230 - class 3 - PG 2 - Methanol
WGK Germany 1
Flash Point(F) 51.8°F
Flash Point(C) 11°C

Documents 

Warnings

Note: These chemicals are for research & laboratory use only. Your order will not be processed if you do not work for, and ship to, a registered laboratory or research facility. Not for topical applications. An official Declaration of Use form may be required.

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WARNING: This product can expose you to chemicals which are known to the State of California to cause cancer and reproductive harm. Prop 65 Warning

Please note: This product is not returnable.

General description Cyclohexane undergoes oxidation in the presence of various oxidants such as hydrogen peroxide, tert-butyl hydroperoxide and molecular oxygen.[2]
Application Cyclohexane has been used to prepare a 1.3M solution of sec-butyllithium.[3] It may be used as a starting Reagent for the synthesis of adipic acid[1] and ε-caprolactam.[1]

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MPN:
343854-5G